Сибирский федеральный университет

Тип публикации: статья из журнала

Год издания: 2000

Аннотация: This paper reports on a procedure for the synthesis of the compound [RuNO(NH3)3Cl(H2O)]Cl2. The complex was studied by IR spectroscopy and X-ray phase and X-ray diffraction analyses. Crystal data for RuCl3N4O2H11: a = 13.151(2), b = 6.852(1), c = 10.361(1) A, V = 933.6(2) A2, space group mathPna2_1/math, Z = 4, dcalc = 2.181 g/cm3, dexp = 2.178 g/cm3. The structure consists of the [RuNO(NH3)3Cl(H2O)]2+ complex cations and Cl- anions. The compound crystallizes as small orange red isometric orthorhombic crystals well soluble in water and insoluble in concentrated hydrochloric acid and organic solvents and is stable when stored in air.

Журнал: Journal of Structural Chemistry

Выпуск журнала: Т. 41, № 6

Номера страниц: 1030-1034

ISSN журнала: 00224766

Место издания: Новосибирск

Издатель: Pleiades Publishing, Ltd. (Плеадес Паблишинг, Лтд)

• Emel'yanov V.A. (Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences eva@che.nsk.su)
• Baidina I.A. (Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences eva@che.nsk.su)
• Gromilov S.A. (Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences eva@che.nsk.su)
• Vasiliev A.D. (L. V. Kirenskii Institute of Physics, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk)
• Belyaev A.V. (Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences eva@che.nsk.su)

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