Сибирский федеральный университет

Тип публикации: доклад, тезисы доклада, статья из сборника материалов конференций

Конференция: Conference on Nanophysics and Nanomaterials, NAN 2019

Год издания: 2020

Идентификатор DOI: 10.4028/www.scientific.net/KEM.854.51

Ключевые слова: derivatography, nanoparticles, transmission electron microscopy, x-ray diffraction, zirconium oxide

Аннотация: The method for synthesis of zirconium oxide nanopowder in low-pressure arc plasma was developed. The physicochemical properties of the nanopowder were studied. The estimation was carried out by means of X-ray diffraction (XRD) and high-resolution transmission electron microscopy (HRTEM). The sequence and kinetics of structural transformations occurring in the specified time-temperature heating regimes have been examined using differential thermal analysis. It was shown that the particles have a nanometer size, a narrow particle size distribution and an amorphous-crystalline structure. The maximum specific surface area detected by the method of sorption of surfactants was 470 m2/g. The issues of crystallization were discussed. From comparison between the results of experimental studies from earlier works with the results obtained for zirconium oxide, it is concluded that the proposed method for producing NPs in a low-pressure arc discharge plasma is universal. © 2020 Trans Tech Publications Ltd, Switzerland.

Журнал: Key Engineering Materials

Выпуск журнала: Vol. 854 KEM

Номера страниц: 51-56

ISSN журнала: 10139826

Издатель: Trans Tech Publications Ltd

• Karpov I.V. (Federal Research Center Krasnoyarsk Scientific Center, Siberian Branch of the Russian Academy of Sciences, 50, Akademgorodok Str, Krasnoyarsk, 660036, Russian Federation, Siberian Federal University, 79, Svobodny ave, Krasnoyarsk, 660041, Russian Federation)
• Ushakov A.V. (Federal Research Center Krasnoyarsk Scientific Center, Siberian Branch of the Russian Academy of Sciences, 50, Akademgorodok Str, Krasnoyarsk, 660036, Russian Federation, Siberian Federal University, 79, Svobodny ave, Krasnoyarsk, 660041, Russian Federation)
• Goncharova E.A. (Siberian Federal University, 79, Svobodny ave, Krasnoyarsk, 660041, Russian Federation)
• Bachurina E.P. (Siberian Federal University, 79, Svobodny ave, Krasnoyarsk, 660041, Russian Federation)
• Shaikhadinov A.A. (Siberian Federal University, 79, Svobodny ave, Krasnoyarsk, 660041, Russian Federation)

• Scopus
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