Inter-laboratory validation of the WDXRF, EDXRF, ICP–MS, NAA and PGAA analytical techniques and geochemical characterisation of obsidian sources in northeast Hokkaido Island, Japan : научное издание | Научно-инновационный портал СФУ

Inter-laboratory validation of the WDXRF, EDXRF, ICP–MS, NAA and PGAA analytical techniques and geochemical characterisation of obsidian sources in northeast Hokkaido Island, Japan : научное издание

Тип публикации: статья из журнала

Год издания: 2018

Идентификатор DOI: 10.1016/j.jasrep.2017.11.013

Ключевые слова: Geochemistry, Hokkaido Island, Obsidian source, Standardisation, Whole-rock analysis

Аннотация: Obsidian provenance studies, based on geochemical signatures, are important for determining the source regions of obsidian artefacts. Such research depends on the availability of reproducible geochemical data. An inter-laboratory study was conducted to validate analytical methods applied to samples from four obsidian sources in northeast Hokkaido Island (Shirataki, Rubeshibe, and Oketo regions). The methods applied were Wavelength-Dispersive X-ray Fluorescence (WDXRF), Energy-Dispersive X-ray Fluorescence (EDXRF), Inductively Coupled Plasma–Mass Spectrometry (ICP–MS), Neutron Activation Analysis (NAA) and Prompt-Gamma Activation Analysis (PGAA). Eight laboratories in Japan, the Russian Federation, Republic Korea, Hungary, Canada, and the USA took part in the trials. Results indicate discrepancies between laboratories, but compositional data for 53 elements were successfully compiled, and reference compositions for 16 elements in each sample defined. Based on these data, a new chemical discrimination scheme is proposed for obsidian sources in the Shirataki, Rubeshibe, and Oketo regions. This scheme is applicable to the discrimination of obsidian sources using semi-quantitative EDXRF analysis, with this being important in non-destructive provenance studies of artefacts. This study fosters the further establishment of reference materials for obsidian sources in the Hokkaido region, and the sharing of such materials. © 2017 Elsevier Ltd

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Издание

Журнал: Journal of Archaeological Science: Reports

Выпуск журнала: Vol. 17

Номера страниц: 379-392

ISSN журнала: 2352409X

Издатель: Elsevier Ltd

Персоны

  • Suda Y. (Department of Geology, Faculty of Education, Nagasaki University, Nagasaki, Japan)
  • Grebennikov A.V. (Far East Geological Institute, Far Eastern Branch of Russian Academy of Sciences, Vladivostok, Russian Federation, Far Eastern Federal University, Vladivostok, Russian Federation)
  • Kuzmin Y.V. (Institute of Geology and Mineralogy, Siberian Branch of Russian Academy of Sciences, Novosibirsk, Russian Federation, Laboratory of Mesozoic and Cenozoic Continental Ecosystems, Tomsk State University, Tomsk, Russian Federation)
  • Glascock M.D. (Research Reactor Center, University of Missouri, Columbia, MO, United States)
  • Wada K. (Hokkaido University of Education, Asahikawa, Hokkaido, Japan)
  • Ferguson J.R. (Research Reactor Center, University of Missouri, Columbia, MO, United States)
  • Kim J.C. (Accelerator Mass Spectrometry Laboratory, Seoul National University, Seoul, South Korea)
  • Popov V.K. (Far East Geological Institute, Far Eastern Branch of Russian Academy of Sciences, Vladivostok, Russian Federation, Far Eastern Federal University, Vladivostok, Russian Federation)
  • Rasskazov S.V. (Institute of the Earth's Crust, Siberian Branch of Russian Academy of Sciences, Irkutsk, Russian Federation)
  • Yasnygina T.A. (Institute of the Earth's Crust, Siberian Branch of Russian Academy of Sciences, Irkutsk, Russian Federation)
  • Saito N. (Palynosurvey Co., Ltd., Fujioka, Gunma Pref., Japan)
  • Takehara H. (Paleo Labo Co., Ltd., Hashima, Gifu Pref., Japan)
  • Carter T. (McMaster Archaeological XRF Laboratory, McMaster University, Hamilton, Ontario, Canada)
  • Kasztovszky Z. (Centre for Energy Research, Hungarian Academy of Sciences, Budapest, Hungary)
  • Biró K.T. (Hungarian National Museum, Budapest, Hungary)
  • Ono A. (Center for Obsidian and Lithic Studies, Meiji University, Tokyo, Japan)

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