Production of Gadolinium Iron Garnet by Anion Resin Exchange Precipitation | Научно-инновационный портал СФУ

Production of Gadolinium Iron Garnet by Anion Resin Exchange Precipitation

Тип публикации: статья из журнала

Год издания: 2019

Идентификатор DOI: 10.1134/S0036023619100127

Ключевые слова: anion-exchange resin, ferrite, nanopowders, synthesis

Аннотация: Abstract—: A new method to synthesize nanosized powders of gadolinium iron garnet was proposed, in which the precipitant is a strong base anion-exchange resin. The effect of the type of the resin (A400 or AV-17-8), the type of its counterion (OH or CO3), and the temperature and duration of the process on the stoichiometry of the formed product and its yield was studied. The time–temperature parameters of gadolinium iron garnet crystallization were determined. The obtained products were investigated by X-ray powder diffraction analysis, thermal analysis, IR spectroscopy, and electron microscopy. Procedures were developed to produce precursors of stoichiometric composition, which, after annealing at 1000°C, form pure phase Gd3Fe5O12 with a particle size of 20–40 nm according to transmission electron microscopy. © 2019, Pleiades Publishing, Ltd.

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Издание

Журнал: Russian Journal of Inorganic Chemistry

Выпуск журнала: Vol. 64, Is. 10

Номера страниц: 1191-1198

ISSN журнала: 00360236

Издатель: Pleiades Publishing

Авторы

  • Saikova S.V. (Russian Acad Sci, Siberian Branch, Fed Res Ctr, Inst Chem & Chem Engn,Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia; Siberian Fed Univ, Krasnoyarsk 660041, RussiaArticle)
  • Kirshneva E.A. (Siberian Fed Univ, Krasnoyarsk 660041, RussiaArticle)
  • Panteleeva M.V. (Russian Acad Sci, Siberian Branch, Fed Res Ctr, Inst Chem & Chem Engn,Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia)
  • Pikurova E.V. (Russian Acad Sci, Siberian Branch, Fed Res Ctr, Inst Chem & Chem Engn,Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia)
  • Evsevskaya N.P. (Russian Acad Sci, Siberian Branch, Fed Res Ctr, Inst Chem & Chem Engn,Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia)

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